Spheroid Nickel Nanoparticles Synthesized in CTAB Solution Using Gamma Radiation

Author:

Ahmad Shahrul Izwan1,Rahim Sapizah2,Shamsudin Siti Aisyah3,Noor An'amt Mohamed4,Ros Fadhlina Che5,Badrudin Fadhlul Wafi1

Affiliation:

1. Universiti Pertahanan Nasional Malaysia

2. Nuclear Malaysia Agency

3. Universiti Kebangsaan Malaysia

4. Universiti Malaysia Kelantan

5. Center for Defence Foundation Studies

Abstract

Pure nickel nanoparticles with some paired grain shaped has been successfully synthesized using gamma radiation technique in aqueous system at ambient temperature without using reducing agent. Cetyl trimethylammonium bromide was used to prevent oxidation during radiolysis process and help to shape the nickel nanoparticles into spheroid. Synthesized nanoparticles were characterized using X-ray diffraction, tunnelling electron microscopy and vibrating sample magnetometer. The particles formed are crystallized with fcc phase without any oxidation state. The particle size ranging from 20 – 50 nm which consists of unique morphology of paired spheroid. Vibrating sample magnetometer analysis shows that sample has ferromagnetic properties with value of magnetic remanence smaller that bulk due to its size.

Publisher

Trans Tech Publications, Ltd.

Subject

Condensed Matter Physics,General Materials Science,Atomic and Molecular Physics, and Optics

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