Preparation and Characterization of Large-Sized ADM Monocrystals-Reference-Cited by-同舟云学术

Preparation and Characterization of Large-Sized ADM Monocrystals

Published:2012-01 Issue: Volume:152-154 Page:126-129
ISSN:1662-7482
Container-title:Applied Mechanics and Materials
language:
Short-container-title:AMM

Author:

Zhang Jun¹,Guo Yan Hui¹

Affiliation:

1. Henan University of Science and Technology

Abstract

Non-agglomerated ammonium dimolybdate (ADM) monocrystals with large diameter and high dispersion has been prepared through reaction-evaporation-crystallization (REC) process using ammonium tetramolybdate and ammonia solution as reactants. The as-prepared ADM monocrystals were systematically characterized by x-ray powder diffraction, transmission-reflection optical microscope, Fourier transform infrared spectroscopy and TG-DSC thermal analysis. It is shown that the as-prepared ADM samples are disperse monocrystals with well grain distribution and geometric shape, which can well meet the quality requirements for the subsequent production of molybdenum powders.

Publisher

Trans Tech Publications, Ltd.

Link

https://www.scientific.net/AMM.152-154.126.pdf

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