Effects of Calcination Parameters on the Microstructure and Morphology of PZT Nanoparticles Prepared by Modified Sol

Effects of Calcination Parameters on the Microstructure and Morphology of PZT Nanoparticles Prepared by Modified Sol–Gel Method

Published:2012-10 Issue: Volume:576 Page:326-329
ISSN:1662-8985
Container-title:Advanced Materials Research
language:
Short-container-title:AMR

Author:

Shakeri Amid¹,Abdizadeh Hossein¹,Golobostanfard Mohammad Reza¹

Affiliation:

1. University of Tehran

Abstract

Lead zirconate titanate nanopowder Pb(Zr0.53Ti0.47)O3 (PZT) was prepared by modified sol-gel method with 1-propanol as solvent and acetylacetone as stabilizer. The microstructure and particle size measurements at different heat treatment conditions were characterized by field emission scanning electron microscopy and x-ray diffraction analysis. It was found that the PZT nanoparticles calcinated at 600 °C showed mean diameter of 75-125 nm with high crystallinity of perovskite-type structure.

Publisher

Trans Tech Publications, Ltd.

Subject

General Engineering

Link

https://www.scientific.net/AMR.576.326.pdf

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