Microstructural Characterization of 66%Co-28%Cr-6%Mo Dental Alloy Powder Obtained by High-Energy Ball Milling

Author:

dos Santos Claudinei1,Habibe Alexandre Fernandes2,Rodrigues Durval3,Minatti José C.3,Lins Jefferson Fabrício C.2,dos Santos Luis Alberto3

Affiliation:

1. Universidade Estadual do Rio de Janeiro

2. UFF-EEIMVR

3. Universidade De são Paulo

Abstract

In this work, the microstructural features of the particles based on 66% Co-28% Cr-6% Mo alloy, were investigated by X-ray diffraction and Scanning electron microscopy (SEM). Powders obtained by high-energy ball milling in an inert atmosphere, and held in SPEX mill with times between 15min and 120min, about ball/powder ratio of 6:1, were characterized by X-ray diffraction indicating in all conditions, Co phase as the crystalline phase of the system. The powders have a morphology that indicate a continuous reduction in average particle size as a function of increasing time, however, the shape of the particles initially flat for times up to 30 minutes, becomes spherodized after 30 minutes of grinding.

Publisher

Trans Tech Publications, Ltd.

Subject

Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science

Reference7 articles.

1. C. Suryanarayana: Progress in Materials Science Vol. 46 (2001), p.1.

2. C.C. Koch: Materials Science and Technology Ð. Vol. 15 (1991), p.193.

3. P.S. Gilman, J.S. Benjamin: Rev. Mater. Sci. Vol. 13 (1983), p.279.

4. DESIGNATION: F 1537 – 08, Standard Specification for Wrought Cobalt-28Chromium-6Molybdenum Alloys for Surgical Implants, (UNS R31537, UNS R31538, and UNS R31539)1.

5. PDF Files, JCPDS Powder Diffraction File, Inorganic materials. Pensilvânia: Swarthmore, International Centre for Diffraction Data., (2010).

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1. Mechanical properties of biocompatible Y-TZP/Al2O3 composites obtained from mechanically alloyed powders;Journal of the Brazilian Society of Mechanical Sciences and Engineering;2020-06-05

2. Co-Cr-Mo-W powder obtained by mechanical alloying;Matéria (Rio de Janeiro);2020

3. Co-Cr-Mo Ternary Phase Diagram Evaluation;MSI Eureka;2017-07-13

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