Analysis of Nanocrystalline Intermetallic Compounds from their X-Ray Diffraction Patterns-Reference-Cited by-同舟云学术

Analysis of Nanocrystalline Intermetallic Compounds from their X-Ray Diffraction Patterns

Published:2010-03 Issue: Volume:644 Page:69-74
ISSN:1662-9752
Container-title:Materials Science Forum
language:
Short-container-title:MSF

Author:

Rojas-Chávez H.¹,Reyes-Carmona Fidel²,Plascencia Gabriel¹,Jaramillo-Vigueras D.¹

Affiliation:

1. Instituto Politécnico Nacional

2. UNAM

Abstract

Synthesis of intermetallic PbSe induced by high-energy ball milling has been studied. Systematic analysis of transformation in the resulting phases of milling from 0 to 10 h has been traced by characterizing the microstructures in terms of morphology, crystallite size, and percentages of phases formed as a function of milling time. Results reveal the formation of two phases. Where the system of PbO-Se transforms gradually to PbSe. Complete transformation is achieved after 10 h of milling time. Study of particle structure by the Rietveld Method further corroborates the value of the nano-order crystallite diameters as evaluated from the microscopic studies.

Publisher

Trans Tech Publications, Ltd.

Subject

Mechanical Engineering,Mechanics of Materials,Condensed Matter Physics,General Materials Science

Link

https://www.scientific.net/MSF.644.69.pdf

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