Structure and Microstructure of Advanced Materials Characterized by Neutron Diffraction

Abstract

Characterization of advanced materials by neutron powder diffraction provides information not accessible by other techniques. Thanks to the low absorption of neutrons, the bulk of the material and large-grain samples can be investigated, moreover in situ at elevated temperatures. The neutron diffraction use is demonstrated on two types of technologically important materials: Ti-Zr alloy and Co-Re high temperature alloy. In Ti-Zr alloy, the residual stress relief and microstrain evolution after ECAP was established. Boron influence on TaC strengthening precipitates in Co-Re high temperature alloys was shown not to be significant at the foreseen alloy operation temperatures, although boron content has a strong influence on the matrix phase.