Technical Note: Methodology Development to Study Two-Dimensional Stainless Steel Pitting Corrosion Mechanisms Using Foil Samples

Author:

Vanegas Mayra1,Wang Ke1,Iannuzzi Mariano1

Affiliation:

1. *Curtin Corrosion Centre, Western Australia School of Mines (WASM), Faculty of Science and Engineering, Curtin University, 6102 Perth, Western Australia, Australia.

Abstract

In this Technical Note, four foil sample preparation methodologies were investigated with “sandwich” like foil electrodes, which enabled the visualization of two-dimensional pit morphologies. The new procedure included the use of nitric acid to prepassivate the foil as the first step; polishing the top layer of the side edges of the foil after the foil was sandwiched in between two glass slides; and immersing the corners in nitric acid before experiments. This new foil sample preparation methodology eliminated pitting artifacts at the corners of the foil samples and provided reliable and reproducible experimental results.

Publisher

Association for Materials Protection and Performance (AMPP)

Subject

General Materials Science,General Chemical Engineering,General Chemistry

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