Use of Silica Gel from Volcanic Ash as Chitosan Composite Membrane’s Filler

Author:

Lubis Maulida1,Sukeksi Lilis1,Harahap Mara Bangun2,Ginting Melva1,Wici Herlinawati1,Ayu Ghendis E1

Affiliation:

1. Department of Chemical Engineering, Faculty of Engineering, University of Sumatera Utara, Almamater Street, Medan, Indonesia

2. Departement of Physics, Faculty of Mathematic and Science, University of Negeri Medan, Medan Estate, North Sumatera 20222, Indonesia

Abstract

This study aims to determine the process of making composite membranes of chitosan and silica fillers from volcanic ash of Sinabung mountain and determine the physical properties of chitosan composite membranes viz. degree of water absorption, functional groups. In this study, composite membranes were made using phase inversion method with the composition of chitosan and silica used were 2 g of chitosan and variations in dosage of fillers 0.6, 0.9 and 1.2 g of silica, while the stirring time was 8, 12 and 16 h. Based on the results , the best membrane conditions were obtained from composite membrane analysis with the best conditions of composite membranes at water absorption is 44.58 %. From the results of FTIR analysis, indicated the presence of OH bonds and Si-O-Si bonds on composite membranes caused by silica gel characteristics of composite membranes also supported by EDX analysis showed composite membrane contained carbon 55.17 %, oxygen 20.36 % and silicon 10.42 %.

Publisher

Asian Journal of Chemistry

Subject

General Chemistry

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