Synthesis and Characterization of Cysteine-Capped CdSe Nanoparticles Using an Alternative of Selenium

Author:

Mokubung K.E.1,Moloto M.J.1,Mubiayi K.P.2,Moloto N.2

Affiliation:

1. Department of Chemistry, Vaal University of Technology, Private Bag X021, Vanderbijlpark, 1900, South Africa

2. School of Chemistry, Faculty of Science, University of the Witwatersrand, Private Bag 3, Johannesburg, 2050, South Africa

Abstract

Present work reports synthesis of L-cysteine capped CdSe nanoparticles at different temperatures via an aqueous medium, non-toxic and green colloidal route. Cadmium chloride (CdCl2·5H2O) and sodium selenite (Na2SeO3) were used as cadmium and selenium sources respectively. The prepared nanoparticles are characterized by UV-visible absorption and photoluminescence spectroscopy, Fourier transform infrared, X-ray diffraction and transmission electron microscopy. The XRD patterns confirm a cubic phase structure of the prepared nanoparticles at 55, 75 and 95 ºC, respectively. The TEM analysis, optical absorption and photoluminescence spectra shows epitaxial growth of CdSe nanoparticles as the temperature increases with average size diameter of 4.12 ± 0.32, 5.02 ± 0.234 and 5.53 ± 0.321 nm for 55, 75 and 95 ºC, respectively.

Publisher

Asian Journal of Chemistry

Subject

General Chemistry

Cited by 1 articles. 订阅此论文施引文献 订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献

1. Effect of L-cysteine capping the CdSe, CdSe:CdS on structural and morphological properties;PHYSICAL MESOMECHANICS OF CONDENSED MATTER: Physical Principles of Multiscale Structure Formation and the Mechanisms of Nonlinear Behavior: MESO2022;2023

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