Structural Regulation and Growth Mechanism of 3D-TiO2 Nanotubes

Author:

Zhang Jing,Xu QinORCID,Xiao Yongna,Duan Sutian,Yin Xiaoguang

Abstract

The microstructure of titanium dioxide nanotubes significantly influences their properties. In this study, two types of three-dimensional titanium dioxide (3D-TiO2) nanotubes with different periodic structures were obtained by periodic pulse anodization of high-purity titanium sheets using discontinuous sawtooth waves under specific alternating-voltage (AV) and alternating-current (AC) conditions, and the inner pores of the nanotubes were both in a “gourd-like” structure. By adjusting the amplitude, period time, and duty cycle of the discontinuous sawtooth wave, the precise regulation of the structure of the 3D-TiO2 inner pore and outer tube can be achieved. This study demonstrates that the formation of “gourd-like” structure of the internal pore is mainly related to the migration rate of ions under low and high voltage/current and the dissolution rate of oxides on the inner wall of nanotubes. This study provides a new prospect for the application of 3D-TiO2 nanotubes, which have great potential for application in sensors, photocatalysis, and other fields.

Funder

the National Natural Science Foundation of China

Publisher

The Electrochemical Society

Subject

Electronic, Optical and Magnetic Materials

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