Micro-Compression Characterization and Thermal Stability of Electrolessly Plated Nickel Phosphorus Alloy

Abstract

The micro-compression characteristic of an electrolessly plated Ni-P alloy was evaluated in this study. Specimens used in the micro-compression test were micro-pillars having a square cross-section fabricated by focused ion beam system. One side of the square cross-section was varied from 5 to 20 μm and the aspect ratio of the micro-pillars was kept at 2:1 to evaluate the sample size effect on the mechanical property. The as-plated Ni-P alloy was amorphous. The sample size effect commonly observed in mechanical properties of metallic micro-specimens was not obvious for micro-pillars fabricated from the as-plated Ni-P alloy, and all of the micro-pillars showed shear band deformation with the 0.2% yield strength at roughly 2.2 GPa. Heat treatment was conducted to study the influence on the sample size effect. After heat treatment at 300 °C for 2 h, an increase in the strength was observed in micro-pillars with all sizes. In addition, for the heat-treated specimens, the fracture strength increased from 3.1 to 4.7 GPa when cross-section of the micro-pillar decreased from 20 × 20 to 10 × 10 μm2, which revealed the sample size effect.