AN ACCESSIBLE GLOVE BOX PROJECT FOR PROCEDURES THAT REQUIRE INERT CONDITIONS

Author:

Pereira Pedro,de Andrade Jean,Maia Pedro,Malpass GeoffroyORCID

Abstract

An inert atmosphere is, in some cases, important for the performing of experiments where substances are toxic and/or sensitive to oxygen. However, the high cost and accessibility of an equipment to work under these conditions, results in the fact that most laboratories do not have this kind of equipment. In this paper, we present a simple and efficient project to build a cheap glove box for processes that require an inert atmosphere. The proposed glove box is made using medium density fiberboard (MDF), an acrylic lid, hinges, air valves, PVC gloves and other materials that can be found easily in local stores or on the internet. Tests to verify the quality of the nitrogen atmosphere were performed using the lighter test and niobium pentachloride (NbCl5), which is a moisture/oxygen sensitive material. The results demonstrated that the equipment is able to maintain an inert atmosphere for several hours, does not permit lighter to function and maintains the NbCl5 stable.

Publisher

Sociedade Brasileira de Quimica (SBQ)

Subject

General Chemistry

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