Synthesis and Characterization of Polypyrrole (PPy) by In-situ Polymerization Technique

Author:

Mrunalini Phalak1,Waghulade Rajendra2,Toda Yogesh3

Affiliation:

1. Department of Applied Physics, Government College of Engineering, Jalgaon – 425 001, Maharastra, India.

2. Department of Physics, D.N.C.V.P's Arts, Commerce & Science College, Jalgaon – 425 001, Maharastra, India.

3. Thin Film Research Lab, Dept. of Physics, Pratap College, Amalner – 425 001, Maharastra, India.

Abstract

This work reports synthesize of polypyrrole nano powder by chemical in-situ polymerization of pyrrole in aqueous solution and ammonium persulfate solution which acts as oxidant. It is characterized by X-ray diffraction (XRD), Fourier infra-red spectroscopy (FTIR) and scanning electron microscopy (SEM). The XRD spectrum reveals that the materials are amorphous in nature. FTIR analysis confirms that all peaks are the main characteristic of PPy. SEM analysis showed that the powder has a uniform granular morphology and the size varies from ∼500 nm to 1 μm. The micrograph of polypyrrole reveals the presence of globular particles. The formed particles are irregular in nature. The results show that the fibers are chemically formed as spherical nanostructures.

Publisher

JACS Directory

Subject

General Medicine

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