New applications for the world’s smallest high-precision capacitance dilatometer and its stress-implementing counterpart

Author:

Küchler R.1ORCID,Wawrzyńczak R.1ORCID,Dawczak-Dębicki H.1ORCID,Gooth J.2,Galeski S.12ORCID

Affiliation:

1. Max Planck Institute for Chemical Physics of Solids 1 , Nöthnitzer Strasse 40, 01187 Dresden, Germany

2. Physikalisches Institut, Universität Bonn 2 , Nussallee 12, D-53115 Bonn, Germany

Abstract

We introduce a new stress dilatometer with exactly the same size and mass as the world’s smallest miniature capacitance dilatometer (height × width × depth = 15 × 14 × 15 mm3, mass: 12 g). To develop this new device, only a single part of the most recently developed mini-dilatometer, the so-called “body,” needs to be replaced. Therefore, the new mini-dilatometer with an interchangeable body can be used for high-resolution measurements of thermal expansion and magnetostriction with and without large stress. We also report two novel applications of both mini-dilatometer cell types. Our new setup was installed for the first time in a cryogen-free system (PPMS DynaCool). The first new setup allows the rotation of both dilatometers in situ at any angle between −90° ≥ μ ≥ +90° in the temperature range from 320 to 1.8 K. We also installed our mini-cells in a dilution refrigerator insert of a PPMS DynaCool, in which dilatometric measurements are now possible in the temperature range from 4 to 0.06 K. Because of the limited sample space, such measurements could not be performed so far. For both new applications, we can resolve the impressive length changes to 0.01 Å.

Funder

Deutsche Forschungsgemeinschaft

Publisher

AIP Publishing

Subject

Instrumentation

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