Contactless characterization of the elastic properties of glass microspheres

Author:

Maire Jeremie1ORCID,Necio Tomasz1ORCID,Chávez-Ángel Emigdio1ORCID,Colombano Martín F.2,Jaramillo-Fernández Juliana3ORCID,Sotomayor-Torres Clivia M.14ORCID,Capuj Nestor E.56,Navarro-Urrios Daniel3ORCID

Affiliation:

1. Catalan Institute of Nanoscience and Nanotechnology (ICN2), CSIC and BIST, Campus UAB 1 , Bellaterra 08193, Barcelona, Spain

2. Université Paris Cité, CNRS, Laboratoire Matériaux et Phénomènes Quantiques 2 , 75013 Paris, France

3. MIND-IN2UB, Departament d'Electrònica, Facultat de Física, Universitat de Barcelona 3 , Martí i Franquès 1 08028, Barcelona, Spain

4. ICREA—Institució Catalana de Recerca i Estudis Avançats 4 , Barcelona 08010, Spain

5. Depto. Física, Universidad de La Laguna 5 , 38200 San Cristóbal de La Laguna, Spain

6. Instituto Universitario de Materiales y Nanotecnología, Universidad de La Laguna 6 , 38071 Santa Cruz de Tenerife, Spain

Abstract

Glass microspheres are of great interest for numerous industrial, biomedical, or standalone applications, but it remains challenging to evaluate their elastic and optical properties in a non-destructive way. In this work, we address this issue by using two complementary contactless techniques to obtain elastic and optical constants of glass microspheres with diameters ranging from 10 to 60 µm. The first technique we employ is Brillouin Light Scattering, which yields scattering with longitudinal acoustic phonons, the frequency of which is found to be 5% lower than that measured in the bulk material. The second technique involves exciting the optical whispering gallery modes of the microspheres, which allows us to transduce some of their vibrational modes. The combined data allow for extracting the refractive index and the elastic constants of the material. Our findings indicate that the values of those properties are reduced with respect to their bulk material counterpart due to an effective decrease of the density, resulting from the fabrication process. We propose the use of this combined method to extract elastic and optical parameters of glass materials in microsphere geometries and compare them with the values of the pristine material from which they are formed.

Funder

Ministerio de Ciencia e Innovación

Ministerio de Asuntos Económicos y Transformacón Digital, Gobierno de España

Horizon 2020 Framework Program

Generalitat de Catalunya

Publisher

AIP Publishing

Subject

General Engineering,General Materials Science

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