1. Division of Materials Science, Institute of Pure and Applied Sciences, University of Tsukuba 1 , Tsukuba, Ibaraki 305-8573, Japan
2. JEOL Ltd. 2 , 3-1-2 Musashino, Akishima, Tokyo 196-8558, Japan
3. Tsukuba Research Center for Energy Materials Science, University of Tsukuba 3 , Tsukuba, Ibaraki 305-8571, Japan