<i>Operando</i> reaction cell for high energy surface sensitive x-ray diffraction and reflectometry-Reference-Cited by-同舟云学术

Operando reaction cell for high energy surface sensitive x-ray diffraction and reflectometry

Published:2022-07-01 Issue:7 Volume:93 Page:073902
ISSN:0034-6748
Container-title:Review of Scientific Instruments
language:en
Short-container-title:Review of Scientific Instruments

Author:

Gleißner R.¹²^ORCID,Beck E. E.¹²^ORCID,Chung Simon¹^ORCID,Semione G. D. L.¹²^ORCID,Mukharamova N.¹^ORCID,Gizer G.³^ORCID,Pistidda C.³^ORCID,Renner D.¹,Noei H.¹^ORCID,Vonk V.¹^ORCID,Stierle A.¹²^ORCID

Affiliation:

1. Centre for X-ray and Nano Science CXNS, Deutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany

2. Fachbereich Physik, Universität Hamburg, Jungiusstraße 9, 20355 Hamburg, Germany

3. Institute of Hydrogen Technology, Materials Technology, Helmholtz-Zentrum hereon GmbH, Max-Planck-Straße 1, 21502 Geesthacht, Germany

Abstract

A proof of concept is shown for the design of a high pressure heterogeneous catalysis reaction cell suitable for surface sensitive x-ray diffraction and x-ray reflectometry over planar samples using high energy synchrotron radiation in combination with mass spectrometry. This design enables measurements in a pressure range from several tens to hundreds of bars for surface investigations under realistic industrial conditions in heterogeneous catalysis or gaseous corrosion studies.

Funder

Helmholtz-Lund International Graduate School

Publisher

AIP Publishing

Subject

Instrumentation

Link

https://aip.scitation.org/doi/pdf/10.1063/5.0098893

Reference31 articles.

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