Large Scale Synthesis of Nickel Oxide (Nio) by Self Propagated Combustion Reaction

Author:

Vijayadarshan P1,Mohan T.1,Viswanath J2,Venugopal K. J3,Rao N. V1,Gupta Amarnath1,Venkataraman A4

Affiliation:

1. R and D center, Premier Explosives Limited, P.O. Peddakandukur-508286, Yadadri District, Telangana, India.

2. Material Chemistry laboratory, Department of Materials Science, Gulbarga University, Kalaburagi-585106, Karnataka. India.

3. Material Chemistry laboratory, Department of Materials Science, Gulbarga University, Kalaburagi-585106,

4. Department of Chemistry, Gulbarga University, Kalaburagi-585106, Karnataka. India.

Abstract

This is a report on large scale synthesis of nickel oxide (NiO) using polyethylene glycol as a fuel employing self-propagating combustion reaction with nickel oxalate as precursor. The synthesized NiO is characterized for its crystal structure, morphology and bonding via XRD, SEM and FTIR respectively. Thermal behavior of the synthesized NiO is studied employing TGA and DSC. Super paramagnetic behavior of the synthesized is studied by magnetic hysteresis.

Publisher

Oriental Scientific Publishing Company

Subject

Pharmacology (medical),Complementary and alternative medicine,Pharmaceutical Science

Reference34 articles.

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