A Facile and Convenient Method to Reduce Organo Azides under Electrochemical Condition and Investigation of the Process thorough Cyclic Voltammetry

Author:

Lona Deena Paliakkara1ORCID,Selvaraj Savariraj Joseph1ORCID,Thomas K Joby2ORCID

Affiliation:

1. 1Department of Chemistry, St. Joseph’s College (Autonomous), Tiruchirappalli- 620 002, Tamil Nadu, India

2. 2Department of Chemistry, St. Thomas’ College (Autonomous), Thrissur- 680 001, Kerala, India.

Abstract

Organo azides are potential precursors for the preparation of amines by different ways of chemical reduction. In the present studies , a simple and more convenient method was developed to reduce to the corresponding amine or sulphonamide under electrochemical condition using sodium ascorbate as the promoter and platinum electrodes. The reduction was achieved with sulfonyl azides, alkyl and aryl azides with moderate to quantitative yields. Cyclic voltametry studies were carried out to study this electrochemical reduction.

Publisher

Oriental Scientific Publishing Company

Subject

Drug Discovery,Environmental Chemistry,Biochemistry,General Chemistry

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