Abstract
In this work a surfactant free microwave method for preparation of Cu2S nanostructure is reported. Cu2S nanostructures (without formation of other phases such as CuS and Cu1.8S) were prepared using Na2SO3 as a weak reducing agent. The effect of different parameters such as time and power of irradiation on the morphology and particle size of the samples have been investigated. The nanostructures were characterized by X-ray diffraction (XRD), energy-dispersive X-ray analysis (EDX), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR), photoluminescence (PL) and ultraviolet-visible (UV-vis) spectroscopy.
Publisher
Iraqi Forum for Intellectuals and Academics
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