Yeni [HNC5H4B(OH)(OCH3)-4]2[Ni(S2C2O2)2] bileşiğinin sentezi ve kristal yapısı

Abstract

In this study, a new compound [HNC5H4B(OH)(OCH3)-4]2[Ni(S2C2O2)2] was synthesized and its crystal structure was determined by the single-crystal X-ray diffraction method. The compound crystallized in the monoclinic crystal system in the P21/n space group. The NiII ion is four-coordinated and has a slightly distorted square-plane geometry. There is NH⋯O, OH⋯O and CH⋯O hydrogen bond interactions in the crystal structure. These interactions form a 3-dimension network stacked along the c axis in the ab plane.