1. Geosciences Department Stony Brook University Stony Brook New York USA
2. ID‐27 European Synchrotron Radiation Facility (ESRF) Grenoble France
3. High Pressure Collaborative Access Team (HP‐CAT), Sector 16, Advanced Photon Source Argonne National Laboratory Argonne Illinois USA
4. GeoSoil and EnviroCARS (GSECARS), Sector 13, Advanced Photon Source Argonne National Laboratory Argonne Illinois USA
5. Chemistry Department Stony Brook University Stony Brook New York USA
6. Also at Geosciences Department, Stony Brook University, Stony Brook, New York, USA.