2-pyrrolidone - capped Mn3O4 nanocrystals-Reference-Cited by-同舟云学术

2-pyrrolidone - capped Mn3O4 nanocrystals

Published:2008-09-01 Issue:3 Volume:6 Page:465-469
ISSN:2391-5420
Container-title:Open Chemistry
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Author:

Özkaya Tevhide¹,Baykal Abdulhadi¹,Toprak Muhammet²

Affiliation:

1. 1Department of Chemistry, Fatih University, 34500 Buyukcekmece, Istanbul, Turkey

2. 2Department of Chemistry and Biochemistry, University of California, Santa Barbara, CA, 93106, USA

Abstract

AbstractWater-soluble Mn3O4 nanocrystals have been prepared through thermal decomposition in a high temperature boiling solvent, 2-pyrrolidone. The final product was characterized with XRD, SEM, TEM, FTIR and Zeta Potential measurements. Average crystallite size was calculated as ∼15 nm using XRD peak broadening. TEM analysis revealed spherical nanoparticles with an average diameter of 14±0.4 nm. FTIR analysis indicated that 2-pyrrolidone coordinates with the Mn3O4 nanocrystals only via O from the carbonyl group, thus confining their growth and protecting their surfaces from interaction with neighboring particles.

Publisher

Walter de Gruyter GmbH

Subject

Materials Chemistry,General Chemistry

Link

http://link.springer.com/content/pdf/10.2478/s11532-008-0041-4.pdf

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