Low temperature synthesis and characterization of Mn3O4 nanoparticles-Reference-Cited by-同舟云学术

Low temperature synthesis and characterization of Mn3O4 nanoparticles

Published:2007-03-01 Issue:1 Volume:5 Page:169-176
ISSN:2391-5420
Container-title:Open Chemistry
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Author:

Baykal Abdülhadi¹,Köseoğlu Yüksel²,Şenel Mehmet¹

Affiliation:

1. 1Department of Chemistry, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey

2. 2Department of Physics, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey

Abstract

AbstractHeating hydrous manganese (II) hydroxide gel at 85 °C for 12 hours produces Mn3O4 nanoparticles. They were characterized by X-ray powder diffraction (XRD) and infrared spectroscopy (FTIR). The particle size estimated from the SEM and X-ray peak broadening is approximately 32 nm, showing them to be nanocrystalline. EPR measurements confirm a typical Mn2+signal with a highly resolved hyperfine structure.

Publisher

Walter de Gruyter GmbH

Subject

Materials Chemistry,General Chemistry

Link

http://link.springer.com/content/pdf/10.2478/s11532-006-0064-7.pdf

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