Synthesis of 4-(2-Hydroxyaryl)-5-Methyl-1,3-Dithiol-2-Thiones-Reference-Cited by-同舟云学术

Synthesis of 4-(2-Hydroxyaryl)-5-Methyl-1,3-Dithiol-2-Thiones

Published:2018-12-01 Issue:2 Volume:26 Page:351-358
ISSN:2067-2446
Container-title:Acta Chemica Iasi
language:en
Short-container-title:

Author:

Bahrin Lucian G.¹

Affiliation:

1. “Petru Poni” Institute of Macromolecular Chemistry , Grigore Ghica Vodă 41A, 700487 , Iasi , Romania

Abstract

Abstract The synthesis of 4-(2-hydroxyaryl)-5-methyl-1,3-dithiol-2-thiones has been accomplished by the reaction of the corresponding 4-(2-hydroxyaryl)-5-methyl-1,3-dithiol-2-ylium perchlorates with sodium sulfide nonahydrate in ethanol at room temperature. The newly obtained derivatives were characterized by NMR and MS spectrometry and IR spectroscopy.

Publisher

Editura Universitatii Alexandru Ioan Cuza din Iasi

Reference31 articles.

1. 1. Ishiguro, T.; Yamaji, K.; Saito, G. Organic Superconductors (Springer Series in Solid-State Sciences), 2nd edition, Ed. Fulde, P., Springer, Berlin, vol. 88, 1998.

2. 2. Ferraris, J.; Cowan, D.O.; Walatka Jr.; V., Perlstein, J.H. Electron transfer in a new highly conducting donor-acceptor complex. J. Am. Chem. Soc.1973, 95, 948-949.

3. 3. Bechgaard, K.; Carneiro, K.; Rasmussen, F.B.; Olsen, M.; Rindorf, G.; Jacobsen, C.S.; Pedersen, H.J.; Scott, J.C. Superconductivity in an organic solid. Synthesis, structure, and conductivity of bis(tetramethyltetraselenafulvalenium) perchlorate, (TMTSF) 2ClO4. J. Am.Chem. Soc.1981, 103, 2440-2442.

4. 4. Yamada, J.; Sugimoto, T. TTF Chemistry - Fundamentals and Applications of Tetrathiafulvalene, Kodansha-Springer, 2004.

5. 5. Buhaceanu, R.; Lungu, N.C.; Forna, N.C.; Asaftei, I.V.; Chirita, P.; Birsa, M.L. The influence of bromine substituent on optical properties of some 1,3-dithiolium derivatives. Rev. Chim. (Bucharest)2013, 64, 960-964.