The Apparatus for Thermomechanical Analysis of Clay-based Ceramics

Author:

Húlan Tomáš1,Štubňa Igor1,Al-Shantir Omar1,Trník Anton1

Affiliation:

1. 1 Constantine the Philosopher University , Department of Physics , A. Hlinku 1, 949 74 Nitra , Slovakia

Abstract

Abstract A dynamic thermomechanical analysis (D-TMA) apparatus is described for measuring the resonant frequency of the flexural vibration and the internal damping of the sample using the impulse excitation technique (IET). Since the measurement is conducted at temperatures up to 1250 °C, an electromagnetic impulser is used for excitation. The free vibrations are registered by an electret microphone, stored and then converted into a frequency spectrum using the fast Fourier transform, from which the resonant frequency can be found. The furnace is built from refractory porous alumina bricks and alumina fiber pads. The heating elements are four SiC rods connected to a temperature controller. The temperature is measured with a Pt-PtRh10 thermocouple in close proximity to the sample.

Publisher

Walter de Gruyter GmbH

Subject

Instrumentation,Biomedical Engineering,Control and Systems Engineering

Reference17 articles.

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4. ASTM. (2001). Standard Test Method for Dynamic Young’s Modulus, Shear Modulus, and Poisson’s Ratio for Advanced Ceramics by Impulse Excitation of Vibration. Standard C1259-01. https://doi.org/10.1520/C1259-01

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