Synthesis of Substituted Cyclooctenes through Cross-Coupling Reactions

Author:

Uraguchi DaisukeORCID,Asano Keisuke1ORCID,Murata Ryuichi2,Yoshida Rakuto1

Affiliation:

1. Institute for Catalysis, Hokkaido University

2. Department of Material Chemistry, Graduate School of Engineering, Kyoto University

Abstract

AbstractCross-coupling methods for the introduction of various substituents onto the olefin moiety of cyclooctenes were developed. A range of 1-substituted cis-cyclooctenes were synthesized. These protocols unlocked routes to previously inaccessible derivatives, permitting the syntheses of cis-cyclooctenes bearing various functional groups. Moreover, the method was applied to the synthesis of a 1,2-disubstituted trans-cyclooctene for the first time, which proved to be a significantly more active organocatalyst than the previously developed monosubstituted trans-cyclooctene.

Funder

Japanese Ministry of Education, Culture, Sports, Science and Technology

Inoue Foundation for Science

Japan Association for Chemical Innovation

Tobe Maki Scholarship Foundation

Novartis Foundation (Japan) for the Promotion of Science

Hitachi Global Foundation

Inamori Foundation

Society of Iodine Science

Japan Society for the Promotion of Science

Publisher

Georg Thieme Verlag KG

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