A single-pot synthesis of 4-hydroxybenzophenones <i>via</i> acid-catalyzed alkoxylation of <i>p</i>-quinone methides followed by DDQ-assisted oxo-demethoxylation-Reference-Cited by-同舟云学术

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A single-pot synthesis of 4-hydroxybenzophenones via acid-catalyzed alkoxylation of p-quinone methides followed by DDQ-assisted oxo-demethoxylation

Published:2023 Issue:39 Volume:47 Page:18419-18429
ISSN:1144-0546
Container-title:New Journal of Chemistry
language:en
Short-container-title:New J. Chem.

Author:

Mahey Jasbir Kaur¹²,Pawara Chunilal B.¹²,Kamble Sumit B.¹²^ORCID

Affiliation:

1. Department of Salt and Marine Chemicals, CSIR-Central Salt and Marine Chemicals Research Institute, Gijubhai Badekha Marg, Waghavadi Road Bhavnagar, Gujarat 364002, India

2. Academy of Scientific and Innovative Research (AcSIR), Ghaziabad 201002, Uttar Pradesh, India

Abstract

A single-pot, two-step approach has been established based on the alkoxylation of p-QMs using readily accessible Amberlyst-15 and DDQ-assisted oxo-demethoxylation to synthesize highly valuable 4-hydroxybenzophenones (81–99%) at room temperature.

Funder

Science and Engineering Research Board

Council of Scientific and Industrial Research, India

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,General Chemistry,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2023/NJ/D3NJ03163B

Reference60 articles.

1. Rational design of carbon-based metal-free catalysts for electrochemical carbon dioxide reduction: A review

2. Carbon-based metal-free catalysts

3. Metal-free nanostructured catalysts: sustainable driving forces for organic transformations

4. Green Chemistry in the Synthesis of Pharmaceuticals

5. Urushiol derivatives as biomass-based photocatalysts for the transition-metal-free synthesis of 1,2-amino alcohols

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