Fast determination of fipronil and its metabolites in seafood using PRiME pass-through cleanup followed by isotope dilution UHPLC-MS/MS
Author:
Affiliation:
1. Department of Chemistry
2. Zhejiang University
3. Hangzhou 310027
4. China
5. Key Laboratory of Health Risk Appraisal for Trace Toxic Chemicals of Zhejiang Province
6. Marine Environmental Monitoring Center of Ningbo
7. SOA
8. Ningbo 315040
Abstract
A simple and effective method based on the PRiME pass-through cleanup procedure followed by UHPLC-MS/MS was developed for analyzing fipronil and its metabolites in seafoods.
Funder
National Natural Science Foundation of China
Natural Science Foundation of Zhejiang Province
Publisher
Royal Society of Chemistry (RSC)
Subject
General Engineering,General Chemical Engineering,Analytical Chemistry
Link
http://pubs.rsc.org/en/content/articlepdf/2018/AY/C8AY00445E
Reference35 articles.
1. PRiME pass-through cleanup for the fast determination of aflatoxins in human serum by using LC-MS/MS
2. Determination of Residues of Fipronil and Its Metabolites in Cauliflower by Using Gas Chromatography-Tandem Mass Spectrometry
3. Simultaneous determination of three pesticides and their metabolites in unprocessed foods using ultraperformance liquid chromatography-tandem mass spectrometry
4. Preliminary efficacy investigations of oral fipronil against Anopheles arabiensis when administered to Zebu cattle ( Bos indicus ) under field conditions
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