Homonuclear decoupling for spectral simplification of carbon-13 enriched molecules in solution-state NMR enhanced by dissolution DNP-Reference-Cited by-同舟云学术

Homonuclear decoupling for spectral simplification of carbon-13 enriched molecules in solution-state NMR enhanced by dissolution DNP

Published:2016 Issue:16 Volume:18 Page:11480-11487
ISSN:1463-9076
Container-title:Physical Chemistry Chemical Physics
language:en
Short-container-title:Phys. Chem. Chem. Phys.

Author:

Chinthalapalli Srinivas¹²³⁴⁵,Bornet Aurélien¹²³⁴,Carnevale Diego¹²³⁴⁶,Jannin Sami¹²³⁴,Bodenhausen Geoffrey¹²³⁴⁷

Affiliation:

1. Institut des sciences et ingénierie chimiques (ISIC)

2. Ecole Polytechnique Fédérale de Lausanne (EPFL)

3. CH-1015 Lausanne

4. Switzerland

5. Department of Chemistry

6. Neuchâtel Platform of Analytical Chemistry (NPAC)

7. École Normale Supérieure-PSL Research University

Abstract

Complex overlapping multiplets due to scalar couplings ⁿJ(¹³C, ¹³C) in fully ¹³C-enriched molecules can be simplified by polychromatic irradiation of selected spins.

Funder

Université de Neuchâtel

École Polytechnique Fédérale de Lausanne

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Link

http://pubs.rsc.org/en/content/articlepdf/2016/CP/C5CP07884A

Reference33 articles.

1. Toward Quantitative Measurements of Enzyme Kinetics by Dissolution Dynamic Nuclear Polarization

2. Influence of a Second Radiofrequency Field on High‐Resolution Nuclear Magnetic Resonance Spectra

3. Homonuclear decoupling and peak elimination in Fourier transform nuclear magnetic resonance

4. Homonuclear broad band decoupling and two‐dimensional J‐resolved NMR spectroscopy

5. Polychromatic Decoupling of a Manifold of Homonuclear Scalar Interactions in Solution-State NMR

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