Sensitivity enhanced 14N/14N correlations to probe inter-beta-sheet interactions using fast magic angle spinning solid-state NMR in biological solids-Reference-Cited by-同舟云学术

Sensitivity enhanced 14N/14N correlations to probe inter-beta-sheet interactions using fast magic angle spinning solid-state NMR in biological solids

Published:2016 Issue:32 Volume:18 Page:22583-22589
ISSN:1463-9076
Container-title:Physical Chemistry Chemical Physics
language:en
Short-container-title:Phys. Chem. Chem. Phys.

Author:

Pandey Manoj Kumar¹²³⁴⁵,Amoureux Jean-Paul⁶⁷⁸⁹¹⁰,Asakura Tetsuo¹¹¹²¹³⁴,Nishiyama Yusuke¹²³⁴⁵

Affiliation:

1. RIKEN CLST-JEOL Collaboration Center

2. RIKEN

3. Yokohama

4. Japan

5. JEOL RESONANCE Inc.

6. Shanghai Key Laboratory of Magnetic Resonance

7. School of Physics and Materials Science

8. East China Normal University

9. Shanghai

10. China

11. Department of Biotechnology

12. Tokyo University of Agriculture and Technology

13. Koganei

Abstract

Sensitivity enhanced proton-detected ¹⁴N/¹⁴N correlation method mediated through accelerated ¹H–¹H spin diffusion at fast magic angle spinning (MAS) solid-state NMR is demonstrated to distinguish inter-beta-sheet interactions in naturally abundant parallel and anti-parallel alanine tripeptides.

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Link

http://pubs.rsc.org/en/content/articlepdf/2016/CP/C6CP03848D

Reference38 articles.

1. Advanced Solid-State NMR Methods for the Elucidation of Structure and Dynamics of Molecular, Macromolecular, and Supramolecular Systems

2. Indirect detection of nitrogen-14 in solid-state NMR spectroscopy

3. Direct detection of nitrogen-14 in solid-state NMR spectroscopy

4. Probing Hydrogen Bonding in Cocrystals and Amorphous Dispersions Using 14N–1H HMQC Solid-State NMR

5. Probing intermolecular interactions and nitrogen protonation in pharmaceuticals by novel 15N-edited and 2D 14N-1H solid-state NMR

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