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Online reaction monitoring by single-scan 2D NMR under flow conditions

Published:2020 Issue:2 Volume:145 Page:478-485
ISSN:0003-2654
Container-title:The Analyst
language:en
Short-container-title:Analyst

Author:

Jacquemmoz Corentin¹²³⁴⁵,Giraud François⁶⁷⁸⁹¹⁰,Dumez Jean-Nicolas¹²³⁴⁵^ORCID

Affiliation:

1. CEISAM

2. CNRS UMR6230

3. Université de Nantes

4. 44300 Nantes

5. France

6. ICSN

7. CNRS UPR2301

8. Univ. Paris Sud

9. Université Paris-Saclay

10. 91190 Gif sur Yvette

Abstract

Single-scan 2D NMR based on spatial encoding can be used to monitor chemical reactions with a flow unit in realistic reaction conditions.

Funder

H2020 European Research Council

Conseil Régional des Pays de la Loire

Agence Nationale de la Recherche

Publisher

Royal Society of Chemistry (RSC)

Subject

Electrochemistry,Spectroscopy,Environmental Chemistry,Biochemistry,Analytical Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2020/AN/C9AN01758E

Reference63 articles.

1. Kinetic Profiling of Catalytic Organic Reactions as a Mechanistic Tool

2. Enamine/Dienamine and Brønsted Acid Catalysis: Elusive Intermediates, Reaction Mechanisms, and Stereoinduction Modes Based on in Situ NMR Spectroscopy and Computational Studies

3. THE ELUCIDATION OF MECHANISMS IN HOMOGENEOUS CATALYSIS

4. Reaction monitoring using online vs tube NMR spectroscopy: seriously different results

5. Real-Time Insights into Biological Events: In-Cell Processes and Protein-Ligand Interactions

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