Film before aggregates: an operando GISAXS study on electrochemically assisted surfactant assembly

Author:

Moehl Gilles E.1ORCID,Fitch Samuel D.1,Cicvarić Katarina2,Han Yisong3,Huang Ruomeng2ORCID,Rawle Jonathan4ORCID,Shao Li1,Beanland Richard3,Bartlett Philip N.1ORCID,Denuault Guy1ORCID,Hector Andrew L.1ORCID

Affiliation:

1. School of Chemistry, University of Southampton, SO17 1BJ, UK

2. School of Electronics and Computer Science, University of Southampton, SO17 1BJ, UK

3. Department of Physics, University of Warwick, CV4 7AL, UK

4. Diamond Light Source Ltd, Harwell Science & Innovation Campus, Didcot, OX11 0DE, UK

Abstract

The process of electrochemically assisted surfactant assembly was followed in real time by grazing incidence small angle X-ray scattering with the aim to deconvolute the formation of mesoporous silica film and unwanted porous particles.

Funder

Engineering and Physical Sciences Research Council

Publisher

Royal Society of Chemistry (RSC)

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