Quantitative UHPSFC-MS analysis of elemental sulfur in mineral oil via derivatisation with triphenylphosphine: application to corrosive sulfur-related power transformer failure-Reference-Cited by-同舟云学术

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Quantitative UHPSFC-MS analysis of elemental sulfur in mineral oil via derivatisation with triphenylphosphine: application to corrosive sulfur-related power transformer failure

Published:2020 Issue:14 Volume:145 Page:4782-4786
ISSN:0003-2654
Container-title:The Analyst
language:en
Short-container-title:Analyst

Author:

Garcia Sérgio B.¹²³⁴,Herniman Julie¹²³⁴,Birkin Peter¹²³⁴^ORCID,Pilgrim James⁵²³⁴,Lewin Paul⁵²³⁴,Wilson Gordon⁶⁷⁸⁴,Langley G. John¹²³⁴,Brown Richard C. D.¹²³⁴^ORCID

Affiliation:

1. School of Chemistry

2. University of Southampton

3. Southampton SO17 1BJ

4. UK

5. The Tony Davies High Voltage Laboratory

6. National Grid

7. National Grid House

8. Warwick CV34 6DA

Abstract

Quantification of elemental sulfur in power transformer mineral oil is achieved using UHPSFCMS analysis of an easily accessible derivative Ph₃PS.

Funder

National Grid

Engineering and Physical Sciences Research Council

Publisher

Royal Society of Chemistry (RSC)

Subject

Electrochemistry,Spectroscopy,Environmental Chemistry,Biochemistry,Analytical Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2020/AN/D0AN00602E

Reference23 articles.

1. M. Heathcote , J & P Transformer Book , 2007 , vol. 13 , p. 40

2. CIGRE Technical Brochure n°378, WG A2.32, 2009 , 1 , 5

3. CIGRE Technical Brochure n°625, WG A2.40, 2016 , 1 , 74

4. IEC 60296, Fluids for Electrotechnical Applications: Unused Mineral Insulating Oils in Electrical Equipment, 2012 , 4 , 14

5. IEC 60422, Supervision and Maintenance Guide for Mineral Insulating Oils in Electrical Equipment, 2013 , 4 , 11

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1. Monitoring Aging of Natural Ester Insulating Fluid using Supercritical Fluid Chromatography-Mass Spectrometry (SFC-MS);2024 IEEE 5th International Conference on Dielectrics (ICD);2024-06-30

2. Multiple Sulfur Corrosion Simulation on the Oil–Paper Insulation System Under Synergistic Electric and Thermal Fields;IEEE Transactions on Dielectrics and Electrical Insulation;2023-04

3. Raman spectroscopy based detection of corrosive sulfur in transformer oil: Method and application;High Voltage;2022-07-21

4. Current state and future perspectives of supercritical fluid chromatography;TrAC Trends in Analytical Chemistry;2022-04

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