Liquid–liquid microextraction of glyphosate, glufosinate and aminomethylphosphonic acid for the analysis of agricultural samples by liquid chromatography

Author:

Marín Javier12345,Campillo Natalia12345,Hernández-Córdoba Manuel12345ORCID,Garrido Isabel6789,Fenoll José6789ORCID,Viñas Pilar12345ORCID

Affiliation:

1. Department of Analytical Chemistry

2. Faculty of Chemistry

3. Regional Campus of International Excellence “Campus Mare Nostrum”

4. University of Murcia

5. E-30100 Murcia

6. Department of Food Quality and Warranty

7. Instituto Murciano de Investigación y Desarrollo Agrario y Alimentario (IMIDA)

8. E-30150 Murcia

9. Spain

Abstract

An ion-pair liquid–liquid microextraction procedure followed by LC tandem mass spectrometry allows a reliable and sensitive determination glyphosate, glufosinate y aminomethylphosphonic acid in agricultural samples.

Funder

Fundación Séneca

Ministerio de Ciencia e Innovación

European Regional Development Fund

Publisher

Royal Society of Chemistry (RSC)

Subject

General Engineering,General Chemical Engineering,Analytical Chemistry

Reference39 articles.

1. Environmental and health effects of the herbicide glyphosate

2. Oxidative Degradation of Glyphosate and Aminomethylphosphonate by Manganese Oxide

3. Glyphosate detection: methods, needs and challenges

4. EC , Regulation (EC) No. 396/2005 of the European Parliament and of the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414 , Off. J. Eur. Commun , 2005 , vol. L 70 , pp. 1–16

5. The role of derivatization techniques in the analysis of glyphosate and aminomethyl-phosphonic acid by chromatography

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