Visible light photoredox catalyzed deprotection of 1,3-oxathiolanes
Author:
Affiliation:
1. State Key Laboratory of Applied Organic Chemistry
2. Department of Chemistry
3. Lanzhou University
4. Lanzhou
5. People's Republic of China
6. Chemical Engineering Institute
7. Northwest Minzu University
Abstract
A mild and efficient visible light photoredox catalyzed aerobic deprotection of 1,3-oxathiolanes using Eosin Y as a photocatalyst is disclosed.
Funder
National Natural Science Foundation of China
Fundamental Research Funds for the Central Universities
Publisher
Royal Society of Chemistry (RSC)
Subject
Organic Chemistry,Physical and Theoretical Chemistry,Biochemistry
Link
http://pubs.rsc.org/en/content/articlepdf/2020/OB/C9OB02517K
Reference29 articles.
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2. Asymmetric syntheses based on 1,3-oxathianes. 2. Synthesis of chiral tertiary .alpha.-hydroxy aldehydes, .alpha.-hydroxy acids, glycols [R1R2C(OH)CH2OH], and carbinols [R1R2C(OH)Me] in high enantiomeric purity.
3. Highly diastereoselective reactions of ytterbium-mediated alkynyllithium and alkynylmagnesium reagents with chiral 2-acyl-1,3-oxathianes: reversal of diastereoselectivity
4. Silica sulfuric acid: A versatile reagent for oxathioacetalyzation of carbonyl compounds and deprotection of 1,3-oxathiolanes
5. Chemoselective Deprotection Of 1,3-Oxathiolanes Using Amberlyst 15 and Glyoxylic Acid under Solvent Free Conditions
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