Synthesis of 4-sulfonyl-1,7-diesters via K2CO3-mediated alkylative debenzoylation of α-sulfonyl o-hydroxyacetophenones with acrylates-Reference-Cited by-同舟云学术

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Synthesis of 4-sulfonyl-1,7-diesters via K₂CO₃-mediated alkylative debenzoylation of α-sulfonyl o-hydroxyacetophenones with acrylates

Published:2024 Issue:6 Volume:22 Page:1194-1204
ISSN:1477-0520
Container-title:Organic & Biomolecular Chemistry
language:en
Short-container-title:Org. Biomol. Chem.

Author:

Chang Meng-Yang¹²³^ORCID,Chen Pin-Hsien¹

Affiliation:

1. Department of Medicinal and Applied Chemistry, Kaohsiung Medical University, Kaohsiung 807, Taiwan

2. Department of Medical Research, Kaohsiung Medical University Hospital, Kaohsiung 807, Taiwan

3. NPUST College of Professional Studies, National Pingtung University of Science and Technology, Pingtung 912, Taiwan

Abstract

A one-pot construction of diverse 4-sulfonyl-1,7-diesters by K2CO3-mediated alkylative debenzoylation of α-sulfonyl o-hydroxyacetophenones with acrylates has been developed.

Funder

Ministry of Science and Technology of the People's Republic of China

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/OB/D3OB01703F

Reference31 articles.

1. A facile synthesis of 1,7-dicarbonyl compounds via three-component Michael addition reactions

2. CuCN catalyzed one pot synthesis of γ-keto diesters: domino double Michael addition followed by Nef reaction

3. One-pot synthesis of symmetric 1,7-dicarbonyl compounds via a tandem radical addition–elimination–addition reaction

4. A Selective and Functional Group-Tolerant Ruthenium-Catalyzed Olefin Metathesis/Transfer Hydrogenation Tandem Sequence Using Formic Acid as Hydrogen Source

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