Nano-mole scale sequential signal assignment by 1H-detected protein solid-state NMR-Reference-Cited by-同舟云学术

Nano-mole scale sequential signal assignment by 1H-detected protein solid-state NMR

Published:2015 Issue:81 Volume:51 Page:15055-15058
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Wang Songlin¹²³⁴,Parthasarathy Sudhakar¹²³⁴,Xiao Yiling¹²³⁴,Nishiyama Yusuke⁵⁶⁷⁸⁹,Long Fei¹²³⁴,Matsuda Isamu¹²³⁴,Endo Yuki⁵⁶⁷,Nemoto Takahiro⁵⁶⁷,Yamauchi Kazuo¹⁰¹¹¹²¹³¹⁴,Asakura Tetsuo¹⁵¹⁶¹⁷⁷,Takeda Mitsuhiro¹⁸¹⁹²⁰⁷,Terauchi Tsutomu²¹²²⁷,Kainosho Masatsune¹⁸¹⁹²⁰⁷²³,Ishii Yoshitaka¹²³⁴²⁴

Affiliation:

1. Department of Chemistry

2. University of Illinois at Chicago

3. Chicago

4. USA

5. JEOL RESONANCE Inc.

6. Akishima

7. Japan

8. RIKEN CLST-JEOL Collaboration Center

9. Kanagawa 230-0045

10. Nuclear Magnetic Resonance Core Lab.

11. King Abdullah University of Science and Technology

12. Thuwal 23955-6900

13. Saudi Arabia

14. School of Science and Technology

15. Department of Biotechnology

16. Tokyo University of Agriculture and Technology 2-24-16

17. Koganei

18. Structure Biology Research Center

19. Graduate School of Science

20. Nagoya

21. SAIL Technologies Inc.

22. Tama

23. Graduate School of Science and Engineering

24. Center for Structural Biology

Abstract

We present a 3D ¹H-detected solid-state NMR (SSNMR) approach for main-chain signal assignments of 10–100 nmol of fully protonated proteins.

Funder

National Institutes of Health

Division of Chemistry

National Institute of General Medical Sciences

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2015/CC/C5CC04618A

Reference19 articles.

1. Sensitivity Enhancement in Solid State 15N NMR by Indirect Detection with High-Speed Magic Angle Spinning

2. Sensitivity Enhancement in Solid-State 13C NMR of Synthetic Polymers and Biopolymers by 1H NMR Detection with High-Speed Magic Angle Spinning

3. Sensitive High Resolution Inverse Detection NMR Spectroscopy of Proteins in the Solid State

4. 15N−H Bond Length Determination in Natural Abundance by Inverse Detection in Fast-MAS Solid-State NMR Spectroscopy

5. Ultrahigh Resolution in Proton Solid-State NMR Spectroscopy at High Levels of Deuteration

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