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Dynamic nuclear polarization at 40 kHz magic angle spinning

Published:2016 Issue:15 Volume:18 Page:10616-10622
ISSN:1463-9076
Container-title:Physical Chemistry Chemical Physics
language:en
Short-container-title:Phys. Chem. Chem. Phys.

Author:

Chaudhari Sachin R.¹²³⁴,Berruyer Pierrick¹²³⁴,Gajan David¹²³⁴,Reiter Christian⁵⁶⁷,Engelke Frank⁵⁶⁷,Silverio Daniel L.⁸⁹¹⁰¹¹,Copéret Christophe⁸⁹¹⁰¹¹,Lelli Moreno¹²¹³¹⁴¹⁵¹⁶,Lesage Anne¹²³⁴,Emsley Lyndon¹⁷¹⁸¹⁹¹¹

Affiliation:

1. Institut de Sciences Analytiques

2. Centre de RMN à Très Hauts Champs

3. Université de Lyon (CNRS/ENS Lyon/UCB Lyon 1)

4. France

5. Bruker Biospin

6. 76287 Rheinstetten

7. Germany

8. ETH Zürich

9. Department of Chemistry

10. CH-8093 Zürich

11. Switzerland

12. University of Florence

13. Chemistry Department

14. Magnetic Resonance Center

15. 50019 Sesto Fiorentino (FI)

16. Italy

17. Institut des Sciences et Ingénierie Chimiques

18. Ecole Polytechnique Fédérale de Lausanne (EPFL)

19. CH-1015 Lausanne

Abstract

DNP-enhanced solid-state NMR spectroscopy is shown to maintain performance over a wide range of sample spinning rates up to 40 kHz.

Funder

European Research Council

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Link

http://pubs.rsc.org/en/content/articlepdf/2016/CP/C6CP00839A

Reference83 articles.

1. Advanced Solid-State NMR Methods for the Elucidation of Structure and Dynamics of Molecular, Macromolecular, and Supramolecular Systems

2. Structure and Dynamics of Membrane Proteins by Magic Angle Spinning Solid-State NMR

3. Frontiers in Solid-State NMR Technology

4. Magic Angle Spinning NMR Spectroscopy: A Versatile Technique for Structural and Dynamic Analysis of Solid-Phase Systems

5. Polarization of Nuclei in Metals

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