Continuous flow oxidation of alkynes with KMnO<sub>4</sub> for the synthesis of 1,2-diketone derivatives-Reference-Cited by-同舟云学术

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Continuous flow oxidation of alkynes with KMnO₄ for the synthesis of 1,2-diketone derivatives

Published:2024 Issue:7 Volume:9 Page:1721-1725
ISSN:2058-9883
Container-title:Reaction Chemistry & Engineering
language:en
Short-container-title:React. Chem. Eng.

Author:

Velichko Viktoria¹²^ORCID,Cambie Dario²^ORCID,Secci Francesco¹^ORCID

Affiliation:

1. Dept. of Chemical and Geological Sciences, Cagliari State University, 09042, Monserrato, Cagliari, Italy

2. Max Planck Institute of Colloids and Interfaces, Biomolecular Systems Department, Am Mühlenberg 1, 14476 Potsdam, Germany

Abstract

A continuous-flow process for the conversion of alkynes to 1,2-diketones and α-keto-carboxylic acids, using KMnO4 as the oxidizing agent, has been developed, ensuring reproducibility and high chemical yields.

Funder

Ministero dell’Istruzione, dell’Università e della Ricerca

Deutscher Akademischer Austauschdienst

Publisher

Royal Society of Chemistry (RSC)

Link

http://pubs.rsc.org/en/content/articlepdf/2024/RE/D3RE00716B

Reference41 articles.

1. The first construction of a 3,6-bridged ellagitannin skeleton with 1C4/B glucose core; synthesis of nonamethylcorilagin

2. Ni(ii)–salt catalyzed activation of primary amine-sp3Cα–H and cyclization with 1,2-diketone to tetrasubstituted imidazoles

3. Total Synthesis of Zaragozic Acid C: Implementation of Photochemical C(sp3)–H Acylation

4. Photochemical Synthesis of anL-Erythrose Building Block and Its use in the Preparation of Methyl 2,3,O-Isopropylidene-?-L-apio-L-furanoside

5. Large-Scale Oxidations in the Pharmaceutical Industry

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