Measurement of 14N quadrupole couplings in biomolecular solids using indirect-detection 14N solid-state NMR with DNP-Reference-Cited by-同舟云学术

Measurement of 14N quadrupole couplings in biomolecular solids using indirect-detection 14N solid-state NMR with DNP

Published:2017 Issue:89 Volume:53 Page:12116-12119
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Jarvis J. A.¹²³⁴,Haies I.⁵²³⁴^ORCID,Lelli M.⁶⁷⁸⁹¹⁰^ORCID,Rossini A. J.⁶⁷⁸⁹¹⁰^ORCID,Kuprov I.⁵²³⁴^ORCID,Carravetta M.⁵²³⁴,Williamson P. T. F.¹²³⁴^ORCID

Affiliation:

1. Biological Sciences

2. University of Southampton

3. Southampton

4. UK

5. Chemistry Department

6. Centre de RMN à Tres Hauts Champs

7. Institut de Sciences Analytiques

8. Université de Lyon (CNRS/ENS Lyon/UCB Lyon1)

9. 69100 Villeurbanne

10. France

Abstract

Insights into protein structure through the determination of ¹⁴N quadrupolar interactions using magic-angle spinning dynamic nuclear polarization NMR.

Funder

FP7 Research infrastructures

Engineering and Physical Sciences Research Council

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2017/CC/C7CC03462H

Reference34 articles.

1. 14N NMR determination of NH bond lengths in solids

2. Probing amide bond nitrogens in solids using 14N NMR spectroscopy

3. Fast Magic-Angle Spinning Three-Dimensional NMR Experiment for Simultaneously Probing H—H and N—H Proximities in Solids

4. 14N Quadrupolar Coupling of Amide Nitrogen and Peptide Secondary Structure As Studied by Solid-State NMR Spectroscopy

5. Rapid Acquisition of14N Solid-State NMR Spectra with Broadband Cross Polarization

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