Determination of seven tetracyclines in milk by dissolvable layered double hydroxide-based solid-phase extraction coupled with high-performance liquid chromatography

Author:

Yang Yi12345ORCID,Zhang Jing56784,Li Yongxin56784,Yin Shuo56784,Jiang Yang984,Sun Chengjun56784ORCID

Affiliation:

1. School of Public Health

2. Southwest Medical University

3. Luzhou 646000

4. China

5. West China School of Public Health

6. West China Fourth Hospital

7. Sichuan University

8. Chengdu 610041

9. Sichuan Center for Disease Control and Prevention

Abstract

A dissolvable layered double hydroxide-based solid-phase extraction combined with high-performance liquid chromatography was developed for the analysis of seven tetracyclines in milk samples.

Funder

Fundamental Research Funds for the Central Universities

Publisher

Royal Society of Chemistry (RSC)

Subject

General Engineering,General Chemical Engineering,Analytical Chemistry

Reference36 articles.

1. An overview of the main foodstuff sample preparation technologies for tetracycline residue determination

2. Dispersive liquid–liquid microextraction based on hydrophobic deep eutectic solvents: Application for tetracyclines monitoring in milk

3. Zeolite imidazolate framework-8 as sorbent for on-line solid-phase extraction coupled with high-performance liquid chromatography for the determination of tetracyclines in water and milk samples

4. U.S. Food and Drug Administration , CFR-Code of Federal Regulations Title 21 , https://www.accessdata.fda.gov/scripts/cdrh/cfdocs/cfcfr/cfrsearch.cfm?cfrpart=556&showfr=1&subpartnode=21:6.0.1.1.18.2 , last time accessed: December 28, 2020

5. Food and Agriculture Organization of the United Nations and World Health Organization , CAC/MRL 2-2017, Maximum Residue Limits (MRLs) and Risk Management Recommendations (RMRs) for Residues of Veterinary Drugs in Foods , 2017

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