Optimization and validation of a two-step method for the determination of polybrominated diphenyl ethers in Croatian house dust samples

Author:

Jagić Karla1234,Dvoršćak Marija1234ORCID,Jurič Andreja5234,Safner Toni67834,Klinčić Darija1234

Affiliation:

1. Biochemistry and Organic Analytical Chemistry Unit

2. Institute for Medical Research and Occupational Health

3. HR-10000 Zagreb

4. Croatia

5. Analytical Toxicology and Mineral Metabolism Unit

6. Department of Plant Breeding, Genetics, Biometrics and Experimentation

7. Faculty of Agriculture

8. University of Zagreb

Abstract

Microwave-assisted extraction was applied as a method for extraction of seven polybrominated diphenyl ether (PBDE) congeners (28, 47, 99, 100, 153, 154, and 183) from house dust samples.

Funder

Hrvatska Zaklada za Znanost

Publisher

Royal Society of Chemistry (RSC)

Subject

General Engineering,General Chemical Engineering,Analytical Chemistry

Reference37 articles.

1. UNEP , Guidance for the inventory of polybrominated diphenyl ethers (PBDEs) listed under the Stockholm Convention on Persistent Organic Pollutants , United Nations Environ. Program , 2017 , vol. 127 , pp. 66–75

2. Design of experiment approach for the optimization of polybrominated diphenyl ethers determination in fine airborne particulate matter by microwave-assisted extraction and gas chromatography coupled to tandem mass spectrometry

3. Determination of polybrominated diphenyl ethers in domestic dust by microwave-assisted solvent extraction and gas chromatography–tandem mass spectrometry

4. PBDE serum concentration and preschool maturity of children from Slovakia

5. US EPA , An Exposure Assessment of Polybrominated Diphenyl Ethers , US EPA , 2010

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