Using fast scanning calorimetry to detect guest-induced polymorphism by irreversible phase transitions in the nanogram scale

Author:

Gataullina Karina V.1234ORCID,Buzyurov Aleksey V.1234ORCID,Ziganshin Marat A.1234ORCID,Padnya Pavel L.1234ORCID,Stoikov Ivan I.1234ORCID,Schick Christoph12345ORCID,Gorbatchuk Valery V.1234ORCID

Affiliation:

1. A.M. Butlerov Institute of Chemistry

2. Kazan Federal University

3. 420008 Kazan

4. Russian Federation

5. Institute of Physics

Abstract

Fast scanning calorimetry with a heating rate of 1000 K s−1 enables successful screening of polymorphs for separate microcrystalline aggregates in thiacalixarene powder.

Publisher

Royal Society of Chemistry (RSC)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

Reference39 articles.

1. J. Bernstein , Polymorphism in Molecular Crystals , Oxford University Press , New York , 2002

2. R. Hilfiker , F.Blatter and M.von Raumer , in Polymorphism: in the Pharmaceutical Industry , ed. R. Hilfiker , Wiley-VCH Verlag GmbH & Co. KGaA , Weinheim, Germany , 2006 , ch. 1, pp. 1–19

3. A practical guide to pharmaceutical polymorph screening & selection

4. Facts and fictions about polymorphism

5. G. Nichols , in Polymorphism: in the Pharmaceutical Industry , ed. R. Hilfiker , Wiley-VCH Verlag GmbH & Co. KGaA , Weinheim, Germany , 2006 , ch. 7, pp. 167–210

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