Accurate experimental characterization of the labile N–Cl bond in N-chloro-N′-(p-fluorophenyl)-benzamidine crystal at 17.5 K-Reference-Cited by-同舟云学术

Accurate experimental characterization of the labile N–Cl bond in N-chloro-N′-(p-fluorophenyl)-benzamidine crystal at 17.5 K

Published:2022 Issue:35 Volume:24 Page:6215-6225
ISSN:1466-8033
Container-title:CrystEngComm
language:en
Short-container-title:CrystEngComm

Author:

Destro Riccardo¹,Barzaghi Mario²,Soave Raffaella³,Roversi Pietro⁴⁵^ORCID,Lo Presti Leonardo¹⁶^ORCID

Affiliation:

1. Università degli Studi di Milano, Department of Chemistry, Via Golgi 19, 20133 Milano, Italy

2. Consiglio Nazionale delle Ricerche (CNR), Piazzale Aldo Moro 7, 00185 Roma, Italy

3. Consiglio Nazionale delle Ricerche (CNR), Istituto di Scienze E Tecnologie Chimiche “Giulio Natta” (SCITEC), Via Golgi 19, 20133 Milano, Italy

4. Consiglio Nazionale delle Ricerche (CNR), Istituto di Biologia e Biotecnologia Agraria (IBBA), Via Bassini 15, 20133 Milano, Italy

5. Leicester Institute of Chemical and Structural Biology and Department of Molecular and Cell Biology, University of Leicester, Henry Wellcome Building, Lancaster Road, Leicester LE1 7HR, UK

6. Istituto Nazionale di Fisica Nucleare (INFN), Laboratori Nazionali di Frascati, Frascati, Italy

Abstract

Very low temperature can preserve the photolabile N–Cl bond in a N-chloro-N-benzamidine derivative long enough to carry on an accurate experimental X-ray charge density study.

Funder

Università degli Studi di Milano

Publisher

Royal Society of Chemistry (RSC)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2022/CE/D2CE00957A

Reference68 articles.

1. H.Winick , in Proceedings of the 1997 Particle Accelerator Conference (Cat. No.97CH36167) , IEEE , 2001 , vol. 1 , pp. 37–41

2. Damages Induced by Synchrotron Radiation-Based X-ray Microanalysis in Chrome Yellow Paints and Related Cr-Compounds: Assessment, Quantification, and Mitigation Strategies

3. Radiation damage and dose limits in serial synchrotron crystallography at cryo- and room temperatures

4. Beam damage of single semiconductor nanowires during X-ray nanobeam diffraction experiments

5. On the role of data quality in experimental charge-density studies

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