A efficient protocol for the synthesis of thioamides in [DBUH][OAc] at room temperature-Reference-Cited by-同舟云学术

A efficient protocol for the synthesis of thioamides in [DBUH][OAc] at room temperature

Published:2018 Issue:1 Volume:8 Page:170-175
ISSN:2046-2069
Container-title:RSC Advances
language:en
Short-container-title:RSC Adv.

Author:

Cao Xian-Ting¹²³⁴⁵^ORCID,Qiao Li⁵⁶⁷⁴,Zheng Hui⁵⁶⁷⁴,Yang Hui-Yong⁵⁶⁷⁴,Zhang Peng-Fei¹²³⁴⁵

Affiliation:

1. College of Pharmaceutical Science

2. Zhejiang University of Technology

3. Hangzhou 310014

4. China

5. College of Material, Chemistry and Chemical Engineering

6. Hangzhou Normal University

7. Hangzhou

Abstract

A novel, simple and eco-friendly method to synthesize thioamides from aryl nitriles and sodium sulfide (Na₂S·9H₂O) catalyzed by 1,8-diazabicyclo[5,4,0]undec-7-enium acetate ([DBUH][OAc]) ionic liquid (IL) at room temperature was developed in this paper.

Publisher

Royal Society of Chemistry (RSC)

Subject

General Chemical Engineering,General Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2018/RA/C7RA11259A

Reference36 articles.

1. Mechanism of thioamide drug action against tuberculosis and leprosy

2. Thioamides as Useful Synthons in the Synthesis of Heterocycles

3. A New Thiazole Synthesis by Cyclocondensation of Thioamides and Alkynyl(Aryl)Iodonium Reagents

4. Synthesis and in-vitro anticancer activity of 3,5-bis(indolyl)-1,2,4-thiadiazoles

5. Building 1,2,4-Thiadiazole: Ten Years of Progress

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