35Cl solid-state NMR of HCl salts of active pharmaceutical ingredients: structural prediction, spectral fingerprinting and polymorph recognition-Reference-Cited by-同舟云学术

35Cl solid-state NMR of HCl salts of active pharmaceutical ingredients: structural prediction, spectral fingerprinting and polymorph recognition

Published:2014 Issue:31 Volume:16 Page:7334-7356
ISSN:1466-8033
Container-title:CrystEngComm
language:en
Short-container-title:CrystEngComm

Author:

Hildebrand Marcel¹²³,Hamaed Hiyam¹²³,Namespetra Andrew M.¹²³,Donohue John M.¹²³,Fu Riqiang⁴⁵,Hung Ivan⁴⁵,Gan Zhehong⁴⁵,Schurko Robert W.¹²³

Affiliation:

1. Department of Chemistry and Biochemistry

2. University of Windsor

3. Windsor, Canada N9B 3P4

4. National High Magnetic Field Laboratory

5. Tallahassee, USA

Abstract

A series of HCl salts of active pharmaceutical ingredients (APIs) have been characterized via³⁵Cl solid-state NMR (SSNMR) spectroscopy and first-principles plane-wave DFT calculations of ³⁵Cl NMR interaction tensors.

Publisher

Royal Society of Chemistry (RSC)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2014/CE/C4CE00544A

Reference104 articles.

1. Solid‐State NMR Studies of Pharmaceutical Systems

2. Thermodynamics of Polymorphs

3. Polymorphism: In the Pharmaceutical Industry , ed. R. Hilfiker , Wiley-VCH , Weinheim, Germany , 2006

4. Scientific Considerations of Pharmaceutical Solid Polymorphism in Regulatory Applications

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