Quantitative and convenient real-time reaction monitoring using stopped-flow benchtop NMR-Reference-Cited by-同舟云学术

Quantitative and convenient real-time reaction monitoring using stopped-flow benchtop NMR

Published:2022 Issue:5 Volume:7 Page:1061-1072
ISSN:2058-9883
Container-title:Reaction Chemistry & Engineering
language:en
Short-container-title:React. Chem. Eng.

Author:

Maschmeyer Tristan¹^ORCID,Yunker Lars P. E.¹,Hein Jason E.¹^ORCID

Affiliation:

1. Department of Chemistry, The University of British Columbia, Vancouver, BC V6T 1Z1, Canada

Abstract

We present a stopped-flow benchtop NMR system (composed of commercially available hardware components) that allows for quantitative reaction monitoring to be completed with relative ease, even with experimentally complex reaction systems.

Funder

University of British Columbia

Bristol-Myers Squibb

Natural Sciences and Engineering Research Council of Canada

Publisher

Royal Society of Chemistry (RSC)

Subject

Fluid Flow and Transfer Processes,Process Chemistry and Technology,Chemical Engineering (miscellaneous),Chemistry (miscellaneous),Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2022/RE/D2RE00048B

Reference55 articles.

1. The More, The Better: Simultaneous In Situ Reaction Monitoring Provides Rapid Mechanistic and Kinetic Insight

2. Seeking universal detectors for analytical characterizations

3. Benchtop NMR Spectroscopy and Spectral Analysis of the cis- and trans-Stilbene Products of the Wittig Reaction

4. Incorporating Benchtop NMR Spectrometers in the Undergraduate Lab: Understanding Resolution and Circumventing Second-Order Effects

5. Benchtop NMR spectroscopy in the analysis of substandard and falsified medicines as well as illegal drugs

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