Silica-surface reorganization during organotin grafting evidenced by 119Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges-Reference-Cited by-同舟云学术

Silica-surface reorganization during organotin grafting evidenced by 119Sn DNP SENS: a tandem reaction of gem-silanols and strained siloxane bridges

Published:2014 Issue:33 Volume:16 Page:17822-17827
ISSN:1463-9076
Container-title:Phys. Chem. Chem. Phys.
language:en
Short-container-title:Phys. Chem. Chem. Phys.

Author:

Conley Matthew P.¹²,Rossini Aaron J.³⁴⁵⁶,Comas-Vives Aleix¹²,Valla Maxence¹²,Casano Gilles⁷⁸⁹¹⁰,Ouari Olivier⁷⁸⁹¹⁰,Tordo Paul⁷⁸⁹¹⁰,Lesage Anne³⁴⁵⁶,Emsley Lyndon³⁴⁵⁶,Copéret Christophe¹²

Affiliation:

1. Department of Chemistry and Applied Biosciences

2. CH-8093 Zürich, Switzerland

3. Centre de RMN à Trés Hauts Champs

4. Institut de Sciences Analytiques (CNRS/ENS Lyon/UCB Lyon 1)

5. Université de Lyon

6. 69100 Villeurbanne, France

7. Aix-Marseille Université

8. CNRS

9. ICR UMR 7273

10. 13397 Marseille Cedex 20, France

Abstract

Bu₃Sn(allyl) reacts with Q₂-geminal disilanols and strained siloxane bridges of partially dehydroxylated silica to yield bipodal species through surface rearrangement.

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Link

http://pubs.rsc.org/en/content/articlepdf/2014/CP/C4CP01973C

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