Enhancing the resolution of 1H and 13C solid-state NMR spectra by reduction of anisotropic bulk magnetic susceptibility broadening-Reference-Cited by-同舟云学术

Enhancing the resolution of 1H and 13C solid-state NMR spectra by reduction of anisotropic bulk magnetic susceptibility broadening

Published:2017 Issue:41 Volume:19 Page:28153-28162
ISSN:1463-9076
Container-title:Phys. Chem. Chem. Phys.
language:en
Short-container-title:Phys. Chem. Chem. Phys.

Author:

Hanrahan Michael P.¹²³⁴⁵,Venkatesh Amrit¹²³⁴⁵,Carnahan Scott L.¹²³⁴⁵,Calahan Julie L.⁶⁷⁸⁴,Lubach Joseph W.⁹¹⁰¹¹¹²⁴^ORCID,Munson Eric J.⁶⁷⁸⁴,Rossini Aaron J.¹²³⁴⁵^ORCID

Affiliation:

1. Iowa State University

2. Department of Chemistry

3. Ames

4. USA

5. US DOE Ames Laboratory

6. University of Kentucky

7. College of Pharmacy

8. Lexington

9. Genentech, Inc.

10. Department of Small Molecule Pharmaceutical Sciences

11. 1 DNA Way

12. South San Francisco

Abstract

2D HETCOR experiments enhance the resolution of ¹H and ¹³C solid-state NMR spectra by reducing anisotropic bulk magnetic susceptibility (ABMS) signal broadening.

Funder

Division of Chemistry

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Link

http://pubs.rsc.org/en/content/articlepdf/2017/CP/C7CP04223J

Reference81 articles.

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2. Solid-state NMR spectroscopy in pharmaceutical research and analysis

3. NMR studies of organic polymorphs & solvates

4. Evolution of solid-state NMR in pharmaceutical analysis

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